甲醇(mL) | 温度(℃) | TMP(g) | 二水合氯化铜(g) | 盐酸羟胺(g) | 压力(atm) | 时间 | 收率% |
10 | 60 | 3 | 0.60 | 0.60 | 5 | 2 h | 84.03 |
10 | 60 | 3 | 0.60 | 0.70 | 5 | 2 h | 85.40 |
10 | 60 | 3 | 0.70 | 0.60 | 5 | 2 h | 85.20 |
10 | 60 | 3 | 0.70 | 0.70 | 5 | 2 h | 84.82 |
10 | 60 | 3 | 0.60 | 0.76 | 5 | 2 h | 85.25 |
10 | 60 | 3 | 0.76 | 0.60 | 5 | 2 h | 85.84 |
10 | 60 | 3 | 0.76 | 0.76 | 15 | 2 h | 89.26 |
10 | 60 | 3 | 0.76 | 0.76 | 15 | 4.5 h | 89.27 |